Use this procedure for hard connectors made from metal (titanium) or ceramics. In the system, these are connections to and from the analytical head of the autosampler (connections to injection valve and needle), and to a metal column.
When tightening a fitting for the first time, start from the finger-tight position (which is not necessarily a vertical wrench position) and rotate the wrench by 135 – 180 °. Staying below 135 ° (grey arrow) will be insufficiently tight, more than 180 ° (red arrow) could damage the capillary.
When tightening the fitting for the second and subsequent times, again start from the finger-tight position (which is not necessarily a vertical wrench position) and rotate the wrench by 90 – 135 °. Staying below 90 ° (grey arrow) could be insufficiently tight, more than 135 ° (red arrow) could damage the capillary.
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id: 3358271115